SMART 6 Microwave + Infrared Moisture & Solids Analyzer Manual THIS PAGE INTENTIONALLY LEFT BLANK Contents Introduction Introduction 1 Safety Safety Notations 2 Notice 3 Instrument Overview Front View 4 Right Side View 4 Left Side View 4 Rear View 5 Instrument Filters 5 Software Overview Software Icons 6 Home Screen 7 Method Screen (One Touch and Classic) 8 System Menu 9 System Installation Unpacking 12 System Setup 14 Sample Analysis Sampling 19 Preparation 19 Weight 19 Glass Fiber Pads 19 Application 19 Perform a Method Perform a Standard Method 21 Perform a Wastewater Method 24 Perform a Syringe Method 24 Perform an Ash Method 25 Perform an iDri Method 25 Method - Create, Edit and Delete Create a One Touch Method 26 Create a Classic Method 32 Create a ProFat Method 37 Edit Method 42 Delete Method 43 Users Create User 44 Edit/Delete User 46 Auto Login 47 Logs 48 Method Import and Export Import 49 Export 50 Data Management SMART 6 Database 52 SMART 6 Statistics 53 SMART 6 Printer Internal Printer Paper Installation 55 Internal Printer 56 External Database and Networks Setup 59 Software Update How to Update Software 61 SMART 6 Maintenance Routine Maintenance 62 One Touch Category Parameters Category Parameters 64 System Specifications Location 65 Instrument Dimensions 65 Electrical Requirements 65 Environmental Constraints 65 Warranty Limited Warranty Information 67 Contact Information CEM Corporation Headquarters 69 CEM International Subsidiaries 69 CEM Distributors 70 1 Introduction Introduction Introduction The SMART 6 TM Analyzer is designed to provide a rapid direct determination of the moisture, or other volatile components, of any and all products. Using a combination of microwave and infrared energy, the SMART 6 is able to accurately analyze samples with moisture content from 0.01-99.99%, as well as samples containing polar or non-polar solvents. The SMART 6 consists of an integrated 4 place balance to 0.1 mg sensitivity for continuous weight monitoring and feedback. SMART 6 utilizes a patented combination of microwave and infrared power, providing the most rapid and complete drying available for the widest range of sample types. Each system includes an infrared sensor for determining sample temperature, USB ports for the transference of data or methods, Ethernet ports for network integration, and a printer option if a paper trail is required. The system is controlled via a 7” TFT-LED glass capacitance touchscreen interface which can accommodate a hierarchy of user logins to protect data and methods and maintain CFR compliance, and is available in multiple languages. Samples are analyzed by first being weighed onto one or two CEM glass fiber samples pads, then heated according to the optimized method parameters, using a combination of the one or both heating sources until the sample stops volatilizing. Results are automatically calculated to provide the final result which is stored in the system for future review. Results can be statistically analyzed by method, date, time, or user on the SMART 6 or transmitted to a LIMS network for real-time data analysis. 2 Safety Safety Safety Notations This manual uses three safety alert words at points in the documentation where the user should be aware of potential hazards. The safety alerts are shown in color-coded boxes. The three words–NOTE, CAUTION, and WARNING–indicate differing levels of observation or action as described below: NOTE A NOTE is intended to provide emphasis of procedures that may be misinterpreted or overlooked, or to otherwise clarify confusing situations. CAUTION A CAUTION is intended to provide essential information and to emphasize procedures which, if not strictly followed, may result in improper instrument operation. WARNING A WARNING is intended to emphasize dangerous or hazardous conditions which may result in personal injury to the user and damage or destruction of the instrument. Safety measures have been installed in the system, ensuring safety and confidence for users. Three interlock switches are utilized to monitor the proper sealing of the system to avoid any possibility of microwave leakage. Flame detection with infrared feedback has been integrated to detect excessive temperature and immediately render the instrument inoperable. If the system is used in a manner not specified by CEM Corporation, these protection devices may be impaired. While the SMART 6 contains numerous safety protocols to protect the end users, certain dangerous situations can arise due to improper handling of hazardous samples and materials. It is critical to the prolonged use of the instrument and the safety of the user that these risks are handled in a safe and responsible manner. WARNING Samples that can be considered flammable, corrosive, poisonous, or explosive must be discussed with the Process Applications group at CEM Corporation prior to analysis in a SMART 6 analyzer. Failure to obtain approval from CEM will void any warranty or service agreement, but more importantly can create a dangerous testing environment. Analyzing solvents or products containing harmful volatiles requires connection of an exhaust hose to the exhaust assembly on the rear of the instrument and leading to an approved fume containment or ventilation system. 3 Safety Beyond validating testing parameters, proper handling of dangerous materials must be followed based on the SDS of the material to further ensure a safe testing environment. Samples which have just been tested should be given adequate time to cool, based on the heat-retention properties of the sample. The cover of the SMART 6 will close on its own once it falls below a certain angle. Keep hands and tools clear of the SMART 6 cavity when closing the cover. Once the cover is closed, do not attempt to place any tools or materials in the cavity while an analysis is being performed. Notice The following precautions should be observed to avoid possible exposure to excessive microwave energy: • Do not tamper with the safety interlocks. The SMART 6 is equipped with three safety interlocks which prevent the instrument from producing microwave power if the cover is open. • Do not place any object between the cavity and the cover or allow soil or cleaner residue to accumulate on sealing surfaces. • Do not operate the instrument if it is damaged. It is particularly important that the instrument cover close properly and that there is no damage to the cover (bent), hinges and latch (broken or loosened), or sealing surfaces. • The instrument should be adjusted or repaired only by qualified service personnel. The following precautions should be observed to avoid instrument-induced electromagnetic interference: • The possibility of instrument-induced electromagnetic interference (EMI) is minimal if precautions outlined above are followed. • The instrument should not be placed close to any electrical device susceptible to EMI. It is suggested that the user post a sign warning pacemaker wearers that a microwave device is in operation. • If the instrument is suspected of inducing EMI, the cover should be carefully inspected. A microwave leakage measurement should be performed as outlined in the Troubleshooting, Maintenance and Service section of this manual. Leakage measured above the legal limit of 5 mW/cm2 should be reported to the CEM Service Department. This instrument utilizes high voltages and microwave radiation. • Instrument service and repair should be performed only by those trained in repair and maintenance of high voltage and microwave power systems. • If the SMART 6 System is used in a manner not specified by CEM Corporation, protection provided by the system may be impaired. 4 Instrument Overview Instrument Overview Front View Cavity Handle Touch Screen Balance Stem Port Cavity Right Side View On/Off Switch Left Side View USB Port Type A (1) Printer (optional) Exhaust Assembly 5 Instrument Overview Rear View Fuses 15A (100-120V) 10A (200-240V) Power Cord Receptacle Magnetron Cooling Fan Ethernet Connection USB Ports Type B (2) USB Ports Type A (3) Instrument Filters Infrared Air Intake Filter Electronics Air Intake Filter Cavity Air Intake Cover (No Filter) 6 Software Overview Software Overview The SMART 6 Moisture/Solids Analyzer utilizes a glass-capacitance touchscreen system. To perform any simple tasks, such as choosing a testing option, opening the system menu, or following the steps to analyze a sample, simply touch the screen where designated and the system will respond. WARNING If the SMART 6 touchscreen is cracked or broken, contact CEM Service immediately because the damaged screen can injure the user, or lead to further system damage. Software Icons Icon Description Icon Description Icon Description Icon Description Advanced Export New Save Back Home ORACLE Search Cursor Import Pause Statistics Delete Information Print System Menu Dilution Key Queue Trac Down Left Revert User Edit Method Right Volume 7 Software Overview Home Screen The Home screen is the first screen that appears when the system is turned on or awoken from the screen saver. Three areas are accessible from this screen - One Touch® Methods, Classic Methods, and System Menu. • One Touch Methods are methods using categories optimized by CEM for a variety of sample types, reducing method development time and effort required by the user. CEM maintains a library of One Touch Methods online. Additional information is available in the installation portion of this manual. • Classic Methods parameters can be revised in the SMART 6, and are typically for users with unique or specialized products that do not provide optimal results using a One Touch Method. Classic methods can be developed on each SMART 6 Analyzer, or imported from another instrument at a separate location. • The System Menu icon provides access to any functionality that does not directly involve analyzing a sample on the SMART 6. NOTE A log-in screen may appear if an administrator turns auto-login to “on” in the “Users” -> “Settings” menu. 8 Software Overview Method Screen (One Touch and Classic) After choosing either the One-Touch Methods or Classic Methods, the method library will appear. Quickly touching the desired method will access the run screen to begin the sample analysis. Long holding (press and hold for 2-3 seconds) a method icon will open several additional options, which are detailed in this manual. Quick Press Long Hold 9 Software Overview System Menu The following is a basic review of each section of the System Menu to be used as a quick guide for locating software items and instrument functions. • Settings –Adjustable system settings unrelated to sample analysis • Tools – Calibration and Diagnostic tools used to ensure proper system functionality • Users – Location for creating and deleting different user accounts, as well as reviewing user logs if necessary • Printing – Printing options and setup • Video – Videos for ensuring proper system handling and usage • Information – System information including serial number, software version, and contact information, etc. Settings • System – Instrument settings for the audio and visual selections of the individual user • Localization – Regional adjustments including language and the preferred date and time format • Date/Time – Location for setting the correct date and time • Run – Adjustment of settings specific to each sample analysis, including sample ID format, test complete indicators, and flame detect temperature, etc. • Method – User editing of the time intervals (1, 15 or 30 minutes) for method parameters such as ramp time, set time, etc. • Data – Information that will be output to the desired database of the customer • Devices – Location for connecting external devices. Eg – external printer, external balance, or bar code reader 10 Software Overview Tools • Diagnostics – A listing of real-time readings of many of the sensors and parts directly related to unit functionality • Calibration – Calibration and validation of the balance, IR temperature sensor, and fan lift offset • System Update – Used for updating software when a new version is released • Networking – IP connection and setup for using the SMART 6 in conjunction with a LIMS Network or Trac instrument • Profat –Appears only when active Users • Settings – Turning ON/OFF auto-login requirements for users • Logs – Audit trail for tracking user movement within the software, including system and method editing • Add User – Addition of a new user login , either as Basic or Administrator user • Users - A list of users currently created on the instrument 11 Software Overview Printing • Settings – Location for turning auto-print ON/OFF, as well as choosing the format data will print in • Add Printer – For users that require an external printer for results • Connected Printer – Settings for the printer currently connected to the instrument Video • Each video can be played in full screen mode, and volume can be adjusted. Information • System – Reference for Serial Number, Software and Firmware versions, and Calibration dates • Contact Us – Contact for CEM Headquarters and Subsidiaries • Legal Notice – Legal information concerning the use and distribution of the SMART 6 and other CEM products • Software Notice – System notification pertaining to the software currently loaded on the system 12 System Installation System Installation Unpacking 1. Select a location that meets requirements as outlined in the Site Preparation Guide (P/N FM0048) or the “Sys- tem Specifications” section of this manual. 2. While unpacking, inspect the box, accessory kit and instrument for damage that may have occurred during shipping. If you notice damage, DO NOT attempt instrument set up. Contact your CEM representative for help. WARNING If any damage to the instrument is noted, do not attempt instrument operation. 3. Remove and verify that all accessories illustrated and listed are included. Glass Fiber Sample Pads (200 ct box) Balance Pan (2) 10 g Weight Balance Stem (2) Pipette (5) Monitor Solution (6 vials) Spatula Sample Press Fuses (2) Documentation •Operation Manual •Monitor Testing Guide •“Importance of Line Voltage” booklet 13 System Installation 4. Remove the foam packaging material from the top of the instrument. 5. Using two (2) people, carefully lift the instrument from the shipping container, using the handholds in the foam to securely hold the instrument. WARNING The SMART 6 weighs 60 pounds (27kg). While it can be safely lifted by a single person, if not lifted and supported properly, a chance of sustaining an injury or damage to the instrument is possible. Using two people to lift the instrument will greatly reduce both risks. 6. Place the instrument on the workbench. 14 System Installation System Setup 1. After removing the shrink wrap from the instrument, gently lift the dark gray cavity handle to lift the cover from the instrument base. 2. Install the balance pan on the balance stem. 3. Carefully install the balance stem into the instrument cavity with the top of the stem flush with the cavity floor. 4. Close the instrument cover. WARNING The cover of the SMART 6 will close once it falls below a certain angle. Keep hands and tools clear of the cavity when closing the cover. 5. Position the SMART 6 to provide access to the back of the instrument. 6. Remove the screw from the exhaust output. Attach the exhaust elbow so that it faces away from the back of the instrument. Install the screw to secure the exhaust elbow. 15 System Installation NOTE If using an exhaust hose for safe ventilation of volatiles, connect the hose to the exhaust elbow prior to attaching the elbow to the instrument. 7. Remove the two (2) fuse holders from the back of the instrument. Install the supplied fuses (15A for 100- 120V or 10A for 200-240V) into the fuse holders and install the holders into the instrument. 8. Plug the power cord into the instrument and the dedicated electrical receptacle. 9. Connect any cables required for an external balance or transmitting data to a LIMS network or other external database. (Directions to properly transmit data are addressed in this manual.) 10. Position the instrument on the workbench facing forward. 11. Locate the power switch on the right side of the instrument and position it in the ON position. NOTE CEM Corporation recommends that the power cord be connected to a dedicated AC power outlet and that the power switch remains in the ON position at all times. After 15 minutes of idle time, the SMART 6 assumes a “sleep” mode. 12. Once the SMART 6 completes the initial powering, the instrument Home Screen will be displayed. 13. System Users can be set up at this time. See the “Users” section of this manual for instructions on creating/ 16 System Installation editing users and auto log-in. 14. Customize system settings. 14.1. Select the System Menu icon in the bottom right corner of the screen to open the menu screen. 14.2. Select Settings. 14.3. Select Localization. 14.4. If English is not the preferred language, select Language to scroll through and select the applicable system language. NOTE If the language is changed, the SMART 6 will reboot once the SAVE icon is selected. 14.5. Select Date Format to enter the desired format for displaying the date (MM/DD/YYYY, DD/MM/YYYY or YYYY/MM/DD). 14.6. Select Time Format to enter the desired format for displaying the time (12 Hour or 24 Hour). 14.7. Select Date/Time, and set the correct Date and Time.